Petroleum Processing and Petrochemicals ›› 2017, Vol. 48 ›› Issue (5): 37-42.

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SYNTHESIS AND CHARACTERIZATION OF SAPO-11 ZEOLITE WITH SPECIAL CRYSTAL STRUCTURE

    

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  • Received:2016-11-01 Revised:2016-11-11 Online:2017-05-12 Published:2017-04-25
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Abstract: A special crystal structure SAPO-11 zeolite was synthesized by using composite template in acidic conditions and characterized by SEM, XRD, FT-IR, NMR, CRF, BET, DTA and TGA techniques. Its isomerization activity for meta-xylene was evaluated in a small scale continuous flow fixed bed. The results were compared with that of the comparative SAPO-11 zeolite made from single template. The crystal morphology characterized by SEM demonstrates the existence of special crystal structure in each crystal of the samples using composite template; in addition, the physicochemical properties of this sieve having high thermal stability and strong acid are different from the comparative one, resulting in high activity for meta-xylene isomerization reaction.

Key words: SAPO-11, composite template, crystal structure, synthesis, characterization.

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