›› 2017, Vol. 48 ›› Issue (6): 98-102.

• 分析与评定 • 上一篇    

催化裂化油浆泵入口过滤器堵塞原因分析

陈帅1,郗艳龙2,付志永2,邹亢1,袁蕙1,卢立军1,徐广通1   

  1. 1. 中国石化石油化工科学研究院
    2. 中国石化石家庄炼化分公司
  • 收稿日期:2016-11-09 出版日期:2017-06-12 发布日期:2017-05-24
  • 通讯作者: 徐广通 E-mail:xugt.ripp@sinopec.com

REASONS OF INLET FILTER CLOGGING OF FCC SLURRY PUMP

  • Received:2016-11-09 Online:2017-06-12 Published:2017-05-24
  • Contact: Xu Guangtong E-mail:xugt.ripp@sinopec.com

摘要: 针对中国石化石家庄炼化分公司催化裂化装置油浆泵入口过滤器频繁堵塞的情况,采用多种表征手段对油浆泵不同位置提取样品的不溶物粒度、热解行为、形貌和元素组成等进行分析,探究沉积油泥的来源与形成方式,分析油浆泵入口过滤器堵塞的原因。结果表明,油浆泵入口处胶泥的组成和氢碳比与油浆泵滤网过滤出的焦块有较大的差异,前者的氢碳比更接近于焦化生焦样品,表明胶泥中的焦炭是高温油浆热生焦的产物。由此判断油浆泵中的沉积胶泥与滤网过滤出的焦块来源不同,油浆泵入口过滤器堵塞的原因是上游工艺条件的改变使进料油浆中出现了较多的小颗粒焦粉,并在泵中逐渐沉积导致堵塞。

关键词: 催化裂化油浆, 油浆泵, 过滤器堵塞, 原因分析

Abstract: Slurry pump is an important part of fluidized catalytic cracking (FCC) unit. The granularity of insoluble particles, pyrolysis behavior, morphology and elemental composition of the samples obtained from different positions in the FCC slurry pump in Shijiazhuang Company were characterized to investigate reasons that caused the clogging of the filter inlet of the slurry pump. Two kinds of cokes were found in the sludge deposition: small size coke powder and block particles. The results show that the small size coke in the sludge deposition of the pump inlet has a similar H/C atom ratio with the coke from coking unit, but significantly different from the coke blocks in the sludge, which is thought to be generated by FCC reaction, indicating that the small size coke powder in the sludge is the product of pyrolysis reactions of high temperature slurry. It is this coke powder produced due to the changes of operation conditions that causes the filter clogging.

Key words: catalytic cracking slurry, slurry pump, filter clogging, cause analysis