Petroleum Processing and Petrochemicals ›› 2013, Vol. 44 ›› Issue (4): 100-104.

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DETERMINATION OF METAL ELEMENTS IN PIPELINE TRANSPORTATION CRUDE OIL BY CRUCIBLE ASHING AND ICP-AES

  

  • Received:2012-06-29 Revised:2012-07-30 Online:2013-04-12 Published:2013-06-05

Abstract: The determination method for 14 kinds of metal elements in pipeline transportation crude oil was established using crucible and ICP-AES. The test results show that quartz crucible is a good choice for ashing crude oil and the suitable ashing conditions for pipeline transportation crude oil are 550 ℃,3hr. And a variety of elements can be detected accurately at the same time with sampling once. The element detection limit of the method is between 0.0006-0.7230 mg/L, RSD <7.0% (except cadmium 28.75%), and the standard recovery rate of 91%-115%.