Petroleum Processing and Petrochemicals ›› 2018, Vol. 49 ›› Issue (12): 34-38.

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CATALYTIC SYNTHESIS OF 1,5-BIS(2-FURANYL)-1,4-PENTADIEN-3-ONE

    

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  • Received:2018-04-17 Revised:2018-07-03 Online:2018-12-12 Published:2019-01-03
  • Contact: Tao Zhiping E-mail:taozp.ripp@sinopec.com
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Abstract: 1,5-bis(2-furanyl)-1,4-pentadien-3-one was synthesized by the aldol condensation reaction of furfural and acetone in inorganic base medium and is identified by FT-IR,1H-NMR and XRD. The optimum conditions for the reaction are: reaction medium of 0.1 mol?L-1 KOH (aq), reaction temperature 20℃, reaction time 10h, the molar ratio of furfural to acetone 2:1. Under the optimum conditions, the yield of product is 98.5 % with a purity of 98%.

Key words: furfural, 1,5-bis(2-furanyl)-1,4-pentadien-3-one, aldol condensation, catalytic conversion

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