石油炼制与化工

• 分析与评定 • 上一篇    

介电谱技术快速测定车用润滑油粘度

管亮 冯新泸 熊刚 谢建安   

  1. 解放军后勤工程学院军事油料应用与管理工程系 后勤工程学院
  • 收稿日期:2007-07-26 修回日期:1900-01-01 出版日期:2008-02-12 发布日期:2008-02-12
  • 通讯作者: 管亮

RAPID DETERMINATION OF THE VISCOSITY OF AUTOMOBILE LUBE OIL BY DIELECTRIC SPECTROSCOPY

Feng Xin-Lu   

  • Received:2007-07-26 Revised:1900-01-01 Online:2008-02-12 Published:2008-02-12

摘要: 分析了介电谱技术测定石油产品质量指标的技术原理。利用主成分分析方法实现了车用润滑油单级油和多级油的分类。采用偏最小二乘法建立了介电谱技术定量快速预测润滑油40℃粘度、100℃粘度的数学模型。其中,40℃粘度预测值与实测值的相关系数为0.9996,预测误差平均值为1.0542;100℃粘度预测值与实测值的相关系数为0.9984,预测误差平均值为0.0942。研究结果表明,介电谱技术能够准确、有效地评价油品的粘度指标。并且,与现存技术相比,其技术优势明显。

关键词: 介电谱, 主成分分析, 偏最小二乘, 粘度, 定量

Abstract: Using dielectric spectroscopy (DS) to analyze petroleum products was introduced. Base on the principle component analysis method the differences between low grade and high grade automobile lube oils were identified. A model was set up using partial least squares (PLS) method to predict the viscosity values of lube oil at 40℃ and 100℃ rapidly. When the number of principle components reached 7, the predicted values and the actual measured data were in good agreement having correlation coefficient of 0.999 6 and 0.998 4 for 40℃ and 100℃, respectively; the average prediction error for 40℃ and 100℃ were 1.054 and 0.094 2, respectively. Results validated that the viscosity of lube oil could be measured by DS accurately and rapidly.

Key words: Dielectric Spectroscopy, Principle Component Analysis, Partial Least Square, Viscosity, Quantitative