石油炼制与化工 ›› 2019, Vol. 50 ›› Issue (7): 47-51.

• 加工工艺 • 上一篇    下一篇

基于催化剂粒度分布分析催化裂化装置催化剂跑损的原因

王迪1,2,孙立强1,2,严超宇1,2,贾梦达1,2,魏耀东1,3   

  1. 1. 中国石油大学(北京)重质油重点实验室
    2. 过程流体过滤与分离技术北京市重点实验室
    3. 中国石油大学(北京)克拉玛依区工学院
  • 收稿日期:2018-09-17 修回日期:2018-11-06 出版日期:2019-07-12 发布日期:2019-07-25
  • 通讯作者: 魏耀东 E-mail:weiyd@cup.edu.cn
  • 基金资助:
    基于颗粒谱分析的循环流化床颗粒循环故障诊断技术的基础研究;FCC旋风分离器故障诊断技术的基础研究

ANALYSIS OF CATALYST LOSS IN FCCU BASED ON PARTICLE SIZE DISTRIBUTION

    

  1.  
  • Received:2018-09-17 Revised:2018-11-06 Online:2019-07-12 Published:2019-07-25
  • Supported by:
     

摘要: 针对某催化裂化装置出现催化剂跑损故障,现场对三级旋风分离器入口进行采样,通过对跑损催化剂进行颗粒粒度分布和扫描电镜分析,探讨催化剂跑损的原因。结果表明,跑损催化剂的粒度分布曲线呈现多峰分布,其中峰值对应的粒径分别为0.8,9,30 μm。造成这种现象的原因,一方面是由于跑损催化剂中存在较严重的摩擦磨损颗粒和冲击破碎颗粒,形成了前2个较小粒径的峰值;另一方面则是由于旋风分离器的分离效率下降,使得跑损催化剂的中位粒径偏高形成了较大粒径的峰值。

关键词: 催化裂化, 催化剂跑损, 原因, 颗粒粒度分布, 旋风分离器

Abstract: In view of the catalyst lost fault in FCCU, the inlet catalyst of the three-stage cyclone separator was sampled on site, and the particle size distribution and the scanning electron microscopy of the lost catalyst were analyzed. The results showed that there were multi-peaks in the particle size distribution curve of the sample, and the particle size corresponding to the peak value was 0.8, 9 and 30 microns, respectively. The first two smaller particle size particles were formed due to serious frictional wear and breakage of particles. On the other hand, because the separation efficiency of the cyclone separator decreases, the higher median particle size of the lost catalyst resulted in the peak of larger particle size.

Key words: FCC, catalyst loss, cause, particle size distribution, cyclone

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