石油炼制与化工 ›› 2024, Vol. 55 ›› Issue (5): 8-13.

• 加工工艺 • 上一篇    下一篇

催化裂化油浆柔性脱固技术(RSFF)侧线试验和工业应用

牛传峰1,龙有2,武文斌3,胡志海1,韩勇4,吴岳林5,邵志才1,方强1   

  1. 1. 中石化石油化工科学研究院有限公司
    2. 中国石化茂名分公司
    3. 上海石油化工股份有限公司
    4. 上海上阳流体科技有限公司
    5. 安徽实华工程技术股份有限公司
  • 收稿日期:2023-06-12 修回日期:2023-12-19 出版日期:2024-05-12 发布日期:2024-05-06
  • 通讯作者: 牛传峰 E-mail:niucf1000@163.com

SIDE-STREAM TEST AND COMMERCIAL APPLICATION OF FLEXIBLE FILTER TECHNOLOGY FOR FCC SLURRY

  • Received:2023-06-12 Revised:2023-12-19 Online:2024-05-12 Published:2024-05-06
  • Contact: Chuan-Feng NIU E-mail:niucf1000@163.com

摘要: 采用催化裂化油浆柔性脱固(RSFF)技术在中国石化上海石油化工股份有限公司5 kt/a油浆脱固侧线试验装置上进行了油浆过滤试验。结果表明:侧线试验中脱固油浆产品收率为90%左右,脱固油浆中(Al+Si)质量分数在10 μg/g左右,RSFF技术可有效脱除粒径小于1 μm的颗粒;在过滤开始阶段,过滤压差快速上升,然后缓慢上升,压差拐点与进料量呈正相关关系;提高再生触发压差可有效延长过滤周期。基于上述试验结果,在茂名外联石化有限公司300 kt/a装置上进行了工业应用试验,结果表明,脱固油浆产品平均收率达到92%以上,脱固油浆中灰分在100 μg/g以下,灰分脱除率达到98%以上。RSFF油浆脱固技术不需要大量物流循环,对设备磨损低,既适用于加工直接来自催化裂化装置的油浆,也适用于加工来自罐区的油浆甚至外购油浆。

关键词: 催化裂化油浆, 柔性, 脱固, 过滤, 侧线试验

Abstract: FCC slurry filtration test was carried out in the 5 kt/a side-stream test unit using the remove solid flexible filter (RSFF) technique in Shanghai Petrochemical Corporation. The results showed that the yield of the de-solid slurry was about 90% and the mass fraction of (Al+Si) in the de-solid slurry was about 10 μg/g. The particle size smaller than 1 μm could be effectively removed by RSFF technology. In the initial stage of filtration, the filtration pressure difference rose rapidly and then slowly. The inflexion of filtration pressure difference had a positively correlation with the feed flow rate. Based on the above results, an industrial application test was carried out in a 300 kt/a unit of Maoming Wailian Petrochemical Company. The results showed that the average yield of the de-solid slurry was over 92%, the ash content in the de-solid slurry was less than 100 μg/g, and the ash removal rate was about 98%. RSFF technology does not need a lot of material circulation and has low wear to equipment. It is suitable for processing slurry directly from FCC unit and even purchased slurry.

Key words: FCC slurry, flexibility, desolidation, filter, side-stream test