石油炼制与化工 ›› 2025, Vol. 56 ›› Issue (2): 59-64.

• 加工工艺 • 上一篇    下一篇

提高超重力油浆脱固工艺液体收率的方案研究

贺安新1,赵福利2,闵正红1,侯俊毅1,古亚坤1   

  1. 1. 中海油惠州石化有限公司
    2. 中海油天津化工研究设计院有限公司
  • 收稿日期:2024-07-22 修回日期:2024-10-01 出版日期:2025-02-12 发布日期:2025-01-16
  • 通讯作者: 贺安新 E-mail:heanx@cnooc.com.cn
  • 基金资助:
    中国海洋石油集团有限公司“三新三化”项目

RESEARCH ON TECHNICAL SCHEME OF INCREASING LIQUID YIELD OF SUPER-GRAVITY SEPARATOR FOR SLURRY DESOLIDIFYING

  • Received:2024-07-22 Revised:2024-10-01 Online:2025-02-12 Published:2025-01-16

摘要: 液体收率是油浆脱固装置的重要指标,直接关系到经济效益和高灰分组分后处理的难度。超重力分离机采用定期排渣的方式将高灰分的渣浆排出,以保证装置稳定运行。为提高油浆脱固过程的液体收率,通过研究产品油浆灰分变化考察了排渣周期、进料流量和油相阻垢剂对排渣量的影响。试验结果表明:超重力分离机排渣周期越长,液体收率越高,但每处理0.4 t油浆必须进行一次排渣,否则将影响装置稳定性;通过加入油相阻垢剂,可有效减轻渣浆在设备内黏附,从而有助于渣浆排出;在油相阻垢剂加剂量(w)为100 μg/g的情况下,排渣周期可延长66.7%,液体收率提高到96.07%,具有较好的经济效益,且不会影响油浆后续利用。

关键词: 超重力分离机, 油浆脱固, 液体收率, 灰分, 渣浆, 阻垢剂

Abstract: Liquid yield is an important index of oil slurry desolidifying device, which is directly related to the economic benefit and the difficulty of post-treatment of high ash components. The super-gravity separator uses regular slagging to discharge the high ash slurry to ensure the stable operation of the device. In order to improve the liquid yield, the effect of slagging period, feed flow rate and oil phase scale inhibitor on slagging amount was proved by studying the change of slurry ash content. The experimental research shows that the longer the slagging period, the higher the liquid yield of the super-gravity separator, but each 0.4 t oil slurry must be discharged once, otherwise the stability of the device will be affected. By adding the oil phase scale inhibitor, the adhesion of slag slurry in the equipment can be effectively reduced, which helps the slag slurry discharge. When the dosage of oil phase scale inhibitor is 100μg/g, the slagging period can be extended by 66.7% and the liquid yield can be increased to 96.07%, which has a good economic benefit and does not affect the subsequent application of the slurry. The experimental results are expected to provide guidance for the subsequent industrial application of the super-gravity separator.

Key words: super-gravity separator, oil slurry desolidifying, liquid yield, ash content, slag slurry, scale inhibitor