石油炼制与化工 ›› 2025, Vol. 56 ›› Issue (1): 167-171.

• 油品与添加剂 • 上一篇    下一篇

中药丸剂塑料球壳外层密封专用蜡的研究开发

吴国江1,夏树斌1,刘青竹2   

  1. 1. 中国石油抚顺石化公司研究院
    2. 中国鞍山海关
  • 收稿日期:2024-05-31 修回日期:2024-09-25 出版日期:2025-01-12 发布日期:2024-12-27
  • 通讯作者: 吴国江 E-mail:wgj_specialwax@sina.cn

PREPARATION OF A SPECIAL WAX FOR SEALING PLASTIC BALL SHELL OF TRADITIONAL CHINESE MEDICINE PILL

  • Received:2024-05-31 Revised:2024-09-25 Online:2025-01-12 Published:2024-12-27

摘要: 研制了一种用于中药丸剂塑料球壳外层密封的专用蜡。将54号全炼石蜡和80号软质微晶蜡的混合物作为基础蜡料,考察各种添加剂对基础蜡料的熔点、运动黏度及其他性能的影响,确定该专用蜡的最佳制备配方为:54号全炼石蜡与80号软质微晶蜡的质量比为9∶1,低相对分子质量聚乙烯、C5加氢石油树脂、乙烯-醋酸乙烯酯共聚物(EVA)、黏度调节助剂A、煤基费-托合成软质蜡、非晶态α-烯烃共聚物(APAO)的加入量(w,以基础蜡料的质量计)分别为1.0%,1.0%,0.5%,3.0%,20%,1.5%。在温度为120 ℃、时间为30 min、搅拌转速为200 r/min的条件下制备的密封专用蜡在40 ℃及-10~-20 ℃下不变形、不龟裂,性能优于参比样品。

关键词: 中药丸, 塑料球壳, 密封蜡, 运动黏度

Abstract: A special wax for sealing the plastic ball shell of the traditional Chinese medicine pill was prepared with excellent performances in deformation-resistance at high temperature and in anti-cracking at low temperature. Taking the mixture of fully refined wax No.54 and slack microcrystalline wax No.80 as base wax, the effects of diferent additives were investigated on the perfomances of the base wax melting point, viscosity and other properties. An optimum formula for preparing the sealing wax was determined that the dosage of low molecular weight polyethylene, C5 petroleum resin, ethylene-vinyl acetate copolymer, auxiliary viscosity modifier A, coal based Fischer-Tropsch synthetic soft wax and amorphous poly alpha olefin was 1%, 1%, 0.5%, 3.0%, 20% and 1.5%, respectively. The special wax prepared under the conditions of 120 ℃, 30 min and stirring speed of 200 r/min has the advantages of nondeformation and non-cracking at 40 ℃ and -10—-20 ℃, is better than the reference sample.

Key words: traditional Chinese medicine pill, platic ball shell, sealing wax, kinematic viscosity