Abstract: The synthetic procedure of a new micro-mesopore material Beta-KIT-6 was described in detail. The materials synthesized were characterized by X-ray diffraction, N2 adsorption-desorption, scanning electron microscope, transmission electron microscope, nuclear magnetic resonance and infrared spectroscopy to understand more clearly the microporous materials Beta-KIT-6, including crystal type, specific surface area and pore size, morphology, channel structure as well as coordination forms of Al species, which laid a strong foundation for future development and application of Beta-KIT-6.