石油炼制与化工 ›› 2014, Vol. 45 ›› Issue (7): 102-106.

• 分析与评定 • 上一篇    

随机称量-煤油稀释-U形振动管法测定重稠油密度

陆克平   

  1. 中国石化安庆分公司检验中心
  • 收稿日期:2013-10-14 修回日期:2014-01-02 出版日期:2014-07-12 发布日期:2014-06-16
  • 通讯作者: 陆克平 E-mail:lkppkl3349@sina.com

DETERMINATION OF DENSITY OF VISCOUS OIL BY RANDOM WEIGHING –KEROSENE DILUTING AND U-SHAPED OSCILLATING TUBE METHOD

  • Received:2013-10-14 Revised:2014-01-02 Online:2014-07-12 Published:2014-06-16

摘要: 从3个方面对重稠油的煤油混合稀释密度测定法进行改进。采用随机称量的煤油和重稠油混合稀释替代其等体积混合稀释,以U形振动管密度法替代手工漂浮密度计法,推导出以质量计量混合的重稠油密度计算公式,并编成程序安装到计算机里,直接输入4个参数值,即可迅速地得到重稠油标准密度值;重稠油与煤油混合近似服从体积加和性规则,以质量比1:1为中心点,在(1:2)~(2:1)的范围内重稠油与煤油稀释均匀,注入U形振荡管密度仪测定混合油的密度,可获得满意的重稠油密度结果;随机称量-煤油稀释-U形振动管法也适合含泡沫重质原油的密度测定;随机称量-煤油稀释-U形振动管法的3次密度测定的标准偏差在0.000 1 g/cm3以下,与直接U形振荡管法的平行性相当,优于漂浮密度计法。

Abstract: The kerosene dilution method for determination of density of heavy viscous oil was improved in three aspects. First, random weighed kerosene and heavy viscous oil was mixed, instead of equal volume mixing method. Second, a digital analyzer consisting of a U-shaped oscillating sample tube was used to replace the manual hydrometer method. Finally, a computational formula for viscous oil density determination were programmed and installed into the computer, by which the viscous oil density can be automatically and quickly determined through directly entering four parameters. It is found that the mixture of kerosene and heavy oil closely obey the volume additivity rule and within (1:2) ~ (2:1) mass ratio scope of heavy oil and kerosene, the density of heavy oil can be obtained satisfactorily by the modified method. The standard deviation for three times density determination is less than 0.000 1 g/cm3, parallel to the result of direct oscillating U tube method, but superior to hydrometer method. The modified method is also suitable for heavy crude oil containing bubble.