石油炼制与化工 ›› 2025, Vol. 56 ›› Issue (8): 7-12.

• 加工工艺 • 上一篇    下一篇

固定床渣油加氢反应器压降上升的原因及对策

邵志才,刘涛,胡大为,戴立顺   

  1. 中石化石油化工科学研究院有限公司
  • 收稿日期:2025-01-13 修回日期:2025-02-07 出版日期:2025-08-12 发布日期:2025-07-28
  • 通讯作者: 邵志才 E-mail:shaozc.ripp@sinopec.com

REASONS AND COUNTERMEASURES FOR PRESSURE DROP INCREASE IN FIXED BED RESIDUE HYDROTREATING REACTOR


  • Received:2025-01-13 Revised:2025-02-07 Online:2025-08-12 Published:2025-07-28

摘要: 分析了A,B,C 3套固定床渣油加氢工业装置反应器压降上升的主要原因,发现:A装置催化剂床层中Fe,Ca,C的沉积导致催化剂床层空隙率逐渐下降,第一反应器压降上升;B装置Ⅰ系列第七周期催化剂床层中Fe、C的沉积导致催化剂床层空隙率逐渐下降,第一反应器压降上升;C装置Ⅰ系列第二周期前置上流式反应器的催化剂床层膨胀率较大,导致顶层催化剂颗粒碰撞催化剂床层上部约翰逊网或出口收集器,内构件压降增加,反应器压降升高,而上流式反应器中催化剂磨擦产生的粉尘或磨细的催化剂进入第二反应器,降低了第二反应器催化剂床层空隙率,使得其压降升高。针对不同反应器压降上升的原因提出延缓压降上升的措施。

关键词: 固定床, 渣油加氢, 滴流床反应器, 上流式反应器, 压降

Abstract: The main reason for the increase in pressure drop in the fixed bed reactor of three units(A,B,C) was analyzed.The analysis results of the spent catalyst from unit A showed that the deposition of Fe, Ca, and C in the catalyst bed layer led to a decrease in the porosity of the catalyst bed layer, and the pressure drop in the first reactor was increased. The analysis results of the spent catalyst from the seventh RUN of the series I of unit B indicated that the deposition of Fe and C in the catalyst bed led to a decrease in the porosity of the catalyst bed, and the pressure drop in the first reactor was increased. The expansion rate of the catalyst bed in up-flow reactor of the series I of unit C was relatively high in the second RUN, and the top catalyst particles would collide with the Johnson net or outlet collector on the upper part of the catalyst bed, resulting in an increase in pressure drop of the internal components and an increase in pressure drop of the reactor. The dust or finely ground catalyst generated by the friction of the catalyst in the up-flow reactor entered the second reactor, reducing the porosity of the catalyst bed and increasing the pressure drop in the second reactor. Corresponding measures were proposed to delay the increase in pressure drop for different reactors based on their main causes.

Key words: fixed bed, residue hydrotreating, trickle bed reactor, up-flow reactor, pressure drop